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ChemInform Abstract: A Convenient Large Scale Synthesis of 1,1-Diphenyl-1-silacyclopent-3- ene.

✍ Scribed by S. MIGNANI; D. DAMOUR; J.-P. BASTART; G. MANUEL

Book ID
112027666
Publisher
John Wiley and Sons
Year
2010
Weight
25 KB
Volume
27
Category
Article
ISSN
0931-7597

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Silabicyclo[3.1.0] hexane 2 obtained from silacyclopent-3-ene 1 by dichlorocarbene addition is useful in the synthesis of ring-expanded products, such as silacyclohexa-2,4-diene 3 and 5-alkoxysilacyclohex-3-enes 5. Catalytic hydrogenation of compound 3 affords silacyclohexane 4. The new heterocycle