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Chloro­(4-methylpiperidine-1-dithio­carbamato-κ2S:S′)(triphenyl­phosphine-κP)palladium(II)

✍ Scribed by Shaheen, Farkhanda ;Najam-Ul-Haq, Muhammad ;Wurst, Klaus ;Badshah, Amin ;Ali, Saqib

Publisher
International Union of Crystallography
Year
2005
Tongue
English
Weight
119 KB
Volume
62
Category
Article
ISSN
1600-5368

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In the title centrosymmetric complex, [Pd(C 6 H 10 NS 2 ) 2 ], the Pd II atom has a square-planar environment with two dithiocarbamate ligands coordinating through their S atoms in a bidentate chelating fashion.

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In the crystal structure of the title complex, [Cu^II^(C~3~H~6~NS~2~)Cl(C~12~H~8~N~2~)], the Cu^II^ atom has a distorted square-pyramidal coordination geometry comprising one __S__,__S__′-bidentate dimethyldithiocarbamate (Me~2~dtc) ligand, one __N__,__N__′-bidentate 1,10-phenanthroline (phen) ligan

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In the title complex, [Sn(C~7~H~6~Cl)~2~(C~7~H~13~N~2~S~2~)Cl], the Sn atom is five-coordinate in a trigonal–bipyramidal geometry. One Sn—S bond is markedly longer than the other for the chelating dithiocarbamate ligand.

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The molecules of the title complex, Et 3 PAu[SC(OMe) N-(C 6 H 4 Cl-4)] or [Au(C 8 H 7 ClNOS)(C 6 H 15 P)], involve the Au atom with linear coordination [Au-P = 2.2584 (10) A ˚, Au-S = 2.3156 (10)A ˚and P-Au-S = 178.32 (4) ] and are linked into centrosymmetric dimers via secondary AuÁ Á ÁS interactio