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Chloro­[2-{1-[N-methyl-N-(4-methyl­benz­yl)amino]eth­yl}ferrocenyl-κ2N,C1](triphenylphosphine-κP)palladium(II)

✍ Scribed by Geng, Feng-Ying ;Xu, Jian ;Wu, Hong-Fei ;Gao, Ren-Qing ;Wang, Hong-Xing

Publisher
International Union of Crystallography
Year
2006
Tongue
English
Weight
137 KB
Volume
62
Category
Article
ISSN
1600-5368

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Chloro­(2-{[N-(4-methoxy­benz­yl)methyl­
Chloro­(2-{[N-(4-methoxy­benz­yl)methyl­amino]meth­yl}ferrocene-κ2N,C1)(triphenyl­phosphine-κP)palladium(II)
✍ Wang, Hong-Xing ;Wu, Hong-Fei ;Gao, Ren-Qing ;Geng, Feng-Ying ;Li, Ying-Jie 📂 Article 📅 2006 🏛 International Union of Crystallography 🌐 English ⚖ 154 KB

In the title compound, [PdCl{Fe(C 5 H 5 )(C 15 H 17 NO)}-(C 18 H 15 P)] or [FePd(C 5 H 5 )(C 15 H 17 NO)Cl(C 18 H 15 P)], the Pd II atom is in a slightly distorted square-planar environment. The dihedral angle between the two cyclopentadienyl rings of the ferrocenyl group is 6.4 (1) .

Chloro­{1-[(1-hydroxy­methyl-2-methyl­pr
Chloro­{1-[(1-hydroxy­methyl-2-methyl­prop­yl)imino­meth­yl]ferrocenyl-κ2C,N}(triphenyl­phosphine-κP)palladium(II) dichloro­methane solvate
✍ Qian, Heng-Yu ;Cui, Xiu-Ling 📂 Article 📅 2006 🏛 International Union of Crystallography 🌐 English ⚖ 192 KB

The asymmetric unit of the title compound, [FePd-(C 5 H 5 )(C 11 H 15 NO)Cl(C 18 H 15 P)]ÁCH 2 Cl 2 , contains two molecular palladium complexes and two dichloromethane solvent molecules. The Pd atoms have approximately square planar configurations. Intermolecular O-HÁ Á ÁCl hydrogen bonds stabilize