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ChemInform Abstract: Structural Characterization of Pb6Sb6Se17.

โœ Scribed by Mehtap Emirdag-Eanes; Joseph W. Kolis

Publisher
John Wiley and Sons
Year
2010
Weight
28 KB
Volume
33
Category
Article
ISSN
0931-7597

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The ternary selenide Pb 6 Sb 6 Se 17 was synthesized hydrothermally from the binaries (PbSe and Sb 2 Se 3 ) and crystallizes in the orthorhombic space group Pbam (a = 15.835(3), b = 24.043(5), c = 4.134(2)A รŠ , Z = 2). The main building blocks of the crystal structure are ribbons made of square pyra

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Se17(NbCl6)2 and Se17(TaBr6)2 -Two New Compounds in the Structure Type Se17(MX6)2. -The novel isotypic title compounds (triclinic, P1, Z = 2) are prepared by reaction of Se, SeX4, and MX5 (X: Cl, M: Nb; X: Br, M: Ta) in SnCl4 and SiBr4, resp., at 150 โ€ข C (evacuated glass ampoules). The black crysta