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ChemInform Abstract: Synthesis and Structure of the Double Oxide Pb6Re6O19.

✍ Scribed by A. M. ABAKUMOV; R. V. SHPANCHENKO; E. V. ANTIPOV


Publisher
John Wiley and Sons
Year
2010
Weight
33 KB
Volume
29
Category
Article
ISSN
0931-7597

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Synthesis and Crystal Structure of Rb 6 Pb 5 Cl 16 . -The hitherto unknown 6:5 phase of title is prepared by reaction of appropriate amounts of RbCl and PbCl 2 (sealed silica tube, 1. 500 β€’ C, 0.5 h, 2. 335 β€’ C, several weeks). Rb 6 Pb 5 Cl 16 crystallizes in the tetragonal space group P4/mbm (pow