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Synthesis and Structure of the Double Oxide Pb6Re6O19

✍ Scribed by A. M. Abakumov; R. V. Shpanchenko; E. V. Antipov

Publisher: John Wiley and Sons
Year: 1998
Tongue: German
Weight: 91 KB
Volume: 624
Category: Article
ISSN: 0372-7874
DOI: 10.1002/(sici)1521-3749(199804)624:4<750::aid-zaac750>3.0.co;2-4

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✦ Synopsis

Pb 6 Re 6 O 19 oxide has been synthesized in a sealed evacuted silica tube and by high-pressure high-temperature technique. Its crystal structure, refined from X-ray powder data (a = 9.3162(1) A Ê , space group Pn3, R I = 0.021, R p = 0.067), is based on a three-dimensional network of Re 2 O 10 groups linked together by corner sharing. The short Re±Re separation inside the Re 2 O 10 groups (2.45 A Ê ) indicates the presence of a metal-metal bonding.

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