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ChemInform Abstract: Synthesis and Characterization of KTh2Se6, KTh2Te6, and CsTh2Se6.

✍ Scribed by E. J. WU; M. A. PELL; J. A. IBERS

Publisher
John Wiley and Sons
Year
2010
Weight
29 KB
Volume
28
Category
Article
ISSN
0931-7597

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Se17(NbCl6)2 and Se17(TaBr6)2 -Two New Compounds in the Structure Type Se17(MX6)2. -The novel isotypic title compounds (triclinic, P1, Z = 2) are prepared by reaction of Se, SeX4, and MX5 (X: Cl, M: Nb; X: Br, M: Ta) in SnCl4 and SiBr4, resp., at 150 β€’ C (evacuated glass ampoules). The black crysta