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ChemInform Abstract: Highly Chemoselective Metal-Free Reduction of Tertiary Amides.

✍ Scribed by Guillaume Barbe; Andre B. Charette

Publisher
John Wiley and Sons
Year
2008
Weight
32 KB
Volume
39
Category
Article
ISSN
0931-7597

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Selective Reduction of Secondary Amides to Amines in the Presence of Tertiary Amides. -The transformation is achieved by reduction of secondary amide moieties bearing an activating Cbz group with hydrides. Catalytic hydrogenation of the resulting hemiacetals removes the hydroxyl and the Cbz group t