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ChemInform Abstract: 1,3-Dipolar Cycloaddition of Nitriles under Microwave Irradiation in Solvent-Free Conditions.

✍ Scribed by A. DIAZ-ORTIZ; E. DIEZ-BARRA; A. DE LA HOZ; A. MORENO; M. J. GOMEZ-ESCALONILLA; A. LOUPY

Book ID
112037655
Publisher
John Wiley and Sons
Year
2010
Weight
30 KB
Volume
27
Category
Article
ISSN
0931-7597

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Synthesis of Oximes, Conversion to Nitrile Oxides and Their Subsequent 1,3-Dipolar Cycloaddition Reactions under Microwave Irradiation and Solvent-Free Reaction Conditions. -Aldoximes and ketoximes (II) are readily synthesized from aldehydes and ketones (I) on Al 2 O 3 under microwave irradiation.

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Aldoximes and ketoximes were readily synthesized from aldehydes and hydroxylamine hydrochloride on Al 2 O 3 without solvent under microwave irradiation. At higher irradiation power, aldoximes dehydrated to nitriles and ketoximes rearranged to amides. Aldoximes reacted in a one-pot reaction with Nchl