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ChemInform Abstract: Heck Reactions under Microwave Irradiation in Solvent-Free Conditions.

✍ Scribed by A. DIAZ-ORTIZ; P. PRIETO; E. VAZQUEZ

Publisher
John Wiley and Sons
Year
2010
Weight
28 KB
Volume
28
Category
Article
ISSN
0931-7597

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Solvent Free Protection of Carbonyl Group under Microwave Irradiation. -The conversion of carbonyl compounds (I) to the corresponding acetals/ketals (III) or dioxolanes (V) is readily achieved by neat KSF clay or PTSA-catalyzed microwave irradiation in the presence of orthoformates, 1,2-ethanediol,