Bis(tetra-n-butylammonium) tetrabromocadmate(II) toluene disolvate
✍ Scribed by Kropidłowska, Anna ;Chojnacki, Jarosław ;Becker, Barbara
- Publisher
- International Union of Crystallography
- Year
- 2006
- Tongue
- English
- Weight
- 265 KB
- Volume
- 62
- Category
- Article
- ISSN
- 1600-5368
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✦ Synopsis
Single-crystal X-ray study T = 100 K Mean (C-C) = 0.007 A Disorder in solvent or counterion R factor = 0.041 wR factor = 0.095 Data-to-parameter ratio = 29.7 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
📜 SIMILAR VOLUMES
Tetra(n-butyl)ammonium nitrite reacts with ‘dichlorophthalocyaninatoruthenium(III) acid’ to yield bis(tetra(n-butyl)ammonium) bisnitrophthalocyaninatoruthenate(II). It crystallizes monoclinic with crystal data: a = 15.114(4) Å, b = 22.34(3) Å, c = 18.206 (11) Å, β = 90.88(5)°; space group P1 21/n 1,
In the title complex, [(C 4 H 9 ) 4 N] 2 [ZnBr 4 ], the Zn II ion is coordinated by four Br atoms, forming a slightly distorted tetrahedral geometry. The Zn-Br bonds range from 2.3986 (11) to 2.4162 (11) A ˚and the Br-Zn-Br angles range from 106.59 (4) to 112.84 (4) . One of the cations is disordere
The receptor of the title compound, C 14 H 36 N + ÁCl À Á-C 20 H 14 N 4 O 6 , binds a chloride anion via two N-HÁ Á ÁCl hydrogen bonds [NÁ Á ÁCl = 3.2367 (14) A ˚and 3.3239 ( 15) ].