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Bis­(penta­chloro­phenyl) di­sulfide

✍ Scribed by Deng, Shun-Liu ;Long, La-Sheng ;Xie, Su-Yuan ;Huang, Rong-Bin ;Zheng, Lan-Sun ;Ng, Seik Weng


Publisher
International Union of Crystallography
Year
2003
Tongue
English
Weight
153 KB
Volume
59
Category
Article
ISSN
1600-5368

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✦ Synopsis


Single-crystal X-ray study T = 298 K Mean '(C±C) = 0.004 A Ê R factor = 0.036 wR factor = 0.099 Data-to-parameter ratio = 16.3 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.


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✍ Meijboom, Reinout ;Muller, Alfred ;Roodt, Andreas 📂 Article 📅 2005 🏛 International Union of Crystallography 🌐 English ⚖ 124 KB

The title compound, trans-[RhCl(C 18 F 15 P) 2 (CO)], crystallizes with one independent molecule in the asymmetric unit. Important geometric parameters are Rh-P = 2.2797 ( 14) and 2.2993 (14) A ˚, Rh-Cl = 2.3642 (12) A ˚, Rh-C = 1.824 (4) A ˚, C-Rh-Cl = 174.12 (13) , P-Rh-C = 91.73 (13) and 93.71 (1