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Bis(acetato-κO)diaqua­bis(1-methyl­imidazole-κN3)cobalt(II)

✍ Scribed by Papánková, Blažena ;Svoboda, Ingrid ;Fuess, Hartmut

Publisher
International Union of Crystallography
Year
2006
Tongue
English
Weight
266 KB
Volume
62
Category
Article
ISSN
1600-5368

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The Co atom of the title compound, [Co(C 8 H 5 O 3 ) 2 (C 3 H 4 N 2 ) 2 -(H 2 O) 2 ], which lies on a centre of inversion, is coordinated by two imidazole and two water molecules, as well as by formylbenzoate groups, in an all-trans octahedral geometry.

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In the title complex, [Cu(C~9~H~6~NO~2~S~2~)~2~(C~3~H~4~N~2~)~2~], the Cu^II^ atom, lying on an inversion centre, is coordinated by two O atoms and two N atoms in a geometry deviating slightly from square planar. Intermolecular hydrogen bonds link the complex molecules into a layer structure.

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The title compound, [Ni(C 8 H 5 O 3 ) 2 (C 3 H 4 N 2 ) 2 (H 2 O) 2 ], is isostructural with the manganese analogue. The Ni atom, which lies on a centre of inversion, is coordinated by two imidazole and two water ligands, as well as by the formylbenzoate groups, in an all-trans octahedral geometry.

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The Mn atom in the title compound, [Mn(C 8 H 5 O 3 ) 2 -(C 3 H 4 N 2 ) 2 (H 2 O) 2 ], is datively linked to the imidazole heterocycles and water molecules, and covalently linked to the substituted benzoate groups in an all-trans octahedral geometry; the Mn atom lies on a center of inversion.

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The Co II centre in the title complex, [Co(C 8 H 7 O 2 ) 2 (C 3 H 4 N 2 ) 2 -(H 2 O)], has a distorted octahedral coordination geometry, involving three O atoms derived from two 4-methylbenzoate ligands, two N atoms from the imidazole ligands and a water molecule. Intermolecular O-HÁ Á ÁO and N-HÁ Á