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Bis­[(3,5-di­methyl­pyrazol-1-yl)­ethyl] di­sulfide

✍ Scribed by Mills, Allison M. ;Chalbot, Marie-Cécile ;Bouwman, Elisabeth ;Spek, Anthony L.

Publisher
International Union of Crystallography
Year
2003
Tongue
English
Weight
212 KB
Volume
59
Category
Article
ISSN
1600-5368

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✦ Synopsis

In the title compound, C 14 H 22 N 4 S 2 , a diethyl disul®de bridge containing an SÐS bond of 2.0396 (6) A Ê connects two 3,5dimethylpyrazole rings via the N1 atoms. The disul®de molecules are linked by weak CÐHÁ Á Á%(pyrazole) interactions into chains that propagate along the b direction.

📜 SIMILAR VOLUMES

Bis­[3-ethyl-1-methyl-5-(2-oxo­thia­zoli
Bis­[3-ethyl-1-methyl-5-(2-oxo­thia­zolidin-3-yl­carbonyl)­pyrazol-4-yl] di­sulfide
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Single-crystal X-ray study T = 295 K Mean '(C±C) = 0.004 A Ê R factor = 0.037 wR factor = 0.097 Data-to-parameter ratio = 10.4 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

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Single-crystal X-ray study T = 298 K Mean '(C±C) = 0.005 A Ê R factor = 0.064 wR factor = 0.213 Data-to-parameter ratio = 15.3 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

Bis(4-formyl-3-methyl-1-phenyl-1H-pyrazo
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Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.003 A Ê R factor = 0.041 wR factor = 0.103 Data-to-parameter ratio = 15.2 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.