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2,6-Bis(3,5-di­methyl­pyrazol-1-yl­methyl)-4-methyl­phenol

✍ Scribed by Yin, Caixia ;Huo, Fangjun ;Gao, Fei ;Guo, Jianping ;Yang, Pin


Publisher
International Union of Crystallography
Year
2003
Tongue
English
Weight
272 KB
Volume
59
Category
Article
ISSN
1600-5368

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(3,5-Di­methyl­pyrazole)[hydridotris(3,5
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Single-crystal X-ray study T = 298 K Mean '(C±C) = 0.005 A Ê R factor = 0.064 wR factor = 0.213 Data-to-parameter ratio = 15.3 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

Bis­[(3,5-di­methyl­pyrazol-1-yl)­ethyl]
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In the title compound, C 14 H 22 N 4 S 2 , a diethyl disul®de bridge containing an SÐS bond of 2.0396 (6) A Ê connects two 3,5dimethylpyrazole rings via the N1 atoms. The disul®de molecules are linked by weak CÐHÁ Á Á%(pyrazole) interactions into chains that propagate along the b direction.

2,6-Bis­[bis­(pyridin-2-yl­methyl)­amino
✍ Bjernemose, Jens K. ;McKenzie, Christine J. 📂 Article 📅 2003 🏛 International Union of Crystallography 🌐 English ⚖ 302 KB

Single-crystal X-ray study T = 180 K Mean '(C±C) = 0.004 A Ê R factor = 0.051 wR factor = 0.138 Data-to-parameter ratio = 13.7 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

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✍ Thamotharan, S. ;Parthasarathi, V. ;Shinge, Prashant S. ;Badami, Bharati ;Raviku 📂 Article 📅 2004 🏛 International Union of Crystallography 🌐 English ⚖ 171 KB

In the title compound, C 19 H 20 N 2 O 5 Á0.19H 2 O, the coumarin moiety is oriented almost perpendicular to the plane of the pyrazole ring. The crystal structure is stabilized by weak intermolecular CÐHÁ Á Á% interactions.