Bis(4-formyl-3-methyl-1-phenyl-1H-pyrazol-5-yl) sulfide
✍ Scribed by Yang, Li-Min ;Wang, Hong-Qing ;Liu, Zhao-Jie ;Song, Hai-Bin
- Publisher
- International Union of Crystallography
- Year
- 2004
- Tongue
- English
- Weight
- 368 KB
- Volume
- 60
- Category
- Article
- ISSN
- 1600-5368
No coin nor oath required. For personal study only.
✦ Synopsis
Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.003 A Ê R factor = 0.041 wR factor = 0.103 Data-to-parameter ratio = 15.2 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
📜 SIMILAR VOLUMES
In the title compound, C 17 H 12 Cl 2 N 2 O 2 , the dihedral angle formed between the dichlorobenzene and pyrazolyl rings is 38.3 (3) , that between the phenyl and pyrazolyl rings is 46.8 (3) , and that between the two benzene rings is 69.4 (3) .
In the title compound, C 14 H 22 N 4 S 2 , a diethyl disul®de bridge containing an SÐS bond of 2.0396 (6) A Ê connects two 3,5dimethylpyrazole rings via the N1 atoms. The disul®de molecules are linked by weak CÐHÁ Á Á%(pyrazole) interactions into chains that propagate along the b direction.