𝔖 Bobbio Scriptorium
✦   LIBER   ✦

Bis­[3-ethyl-1-methyl-5-(2-oxo­thia­zolidin-3-yl­carbonyl)­pyrazol-4-yl] di­sulfide

✍ Scribed by Tan, Cheng-Xia ;Gu, Jian-Ming ;Shen, De-Long ;Weng, Jian-Quan ;Fan, De-Fang

Publisher
International Union of Crystallography
Year
2004
Tongue
English
Weight
154 KB
Volume
60
Category
Article
ISSN
1600-5368

No coin nor oath required. For personal study only.

✦ Synopsis

Single-crystal X-ray study T = 295 K Mean '(C±C) = 0.004 A Ê R factor = 0.037 wR factor = 0.097 Data-to-parameter ratio = 10.4

For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

📜 SIMILAR VOLUMES

Bis­[(3,5-di­methyl­pyrazol-1-yl)­ethyl]
Bis­[(3,5-di­methyl­pyrazol-1-yl)­ethyl] di­sulfide
✍ Mills, Allison M. ;Chalbot, Marie-Cécile ;Bouwman, Elisabeth ;Spek, Anthony L. 📂 Article 📅 2003 🏛 International Union of Crystallography 🌐 English ⚖ 212 KB

In the title compound, C 14 H 22 N 4 S 2 , a diethyl disul®de bridge containing an SÐS bond of 2.0396 (6) A Ê connects two 3,5dimethylpyrazole rings via the N1 atoms. The disul®de molecules are linked by weak CÐHÁ Á Á%(pyrazole) interactions into chains that propagate along the b direction.

2-Phenyl-3-{5-[3-(trifluoro­meth­yl)phen
2-Phenyl-3-{5-[3-(trifluoro­meth­yl)phen­yl]-1,3,4-thia­diazol-2-yl}­thia­zolidin-4-one
✍ Wan, Rong ;Wu, Feng ;Han, Feng ;Cao, Lin ;Wang, Jin-Tang 📂 Article 📅 2006 🏛 International Union of Crystallography 🌐 English ⚖ 183 KB

The title compound, C 18 H 12 F 3 N 3 OS 2 , was synthesized by the reaction of [(Z)-1-phenylmethylidene]{5-[3-(trifluoromethyl)phenyl]-1,3,4-thiadiazol-2-yl}amine and mercaptoacetic acid. In the structure there are intramolecular C-HÁ Á ÁS and C-HÁ Á ÁN and intermolecular C-HÁ Á ÁN hydrogen bonds.

2-(4-Chloro­phen­yl)-3-[5-(4-methoxy­phe
2-(4-Chloro­phen­yl)-3-[5-(4-methoxy­phen­yl)-1,3,4-thia­diazol-2-yl]thia­zolidin-4-one
✍ Wan, Rong ;Guan, Jianning ;Han, Feng ;Wu, Feng ;Wang, Jin-Tang 📂 Article 📅 2006 🏛 International Union of Crystallography 🌐 English ⚖ 146 KB

In the title compound, C 18 H 14 ClN 3 O 2 S 2 , the thiazolidine ring adopts an envelope conformation. There are intermolecular C-HÁ Á ÁO interactions, forming centrosymmetric dimers.