✦ LIBER ✦

Asymmetric Synthesis of 2-Alkylcyclohexanones on Solid Phases

✍ Scribed by Dr. Paul M. Worster; Dr. Colin R. McArthur; Dr. Clifford C. Leznoff

Publisher: John Wiley and Sons
Year: 1979
Tongue: English
Weight: 242 KB
Volume: 18
Category: Article
ISSN: 0044-8249
DOI: 10.1002/anie.197902211

No coin nor oath required. For personal study only.

✦ Synopsis

field desorption mass spectrum (m/e= 206 for CpV(NO):)[41; in nitromethane solution it behaves as a 1 : 1 electrolyte. The pronounced electron deficit at the central metal of ( I ) is reflected in the high v(N0) frequencies in the IR spectrum and in the strong deshielding of the cyclopentadienyl protons in the 'H-NMR spectrum. Table 1 shows the characteristic spectroscopic data of the cations ( I ) and (2)['l and of the corresponding neutral complexes from which they can be obtained by reaction with NOPF6. Table 1. 1R and 'H-NMR data [a]. Complex IR P I 'H-NMR [c]

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