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Application of the attached proton test technique in 31P NMR spectroscopy

✍ Scribed by H. Jancke; R. Radeglia; J. Neels; A. Porzel

Publisher: John Wiley and Sons
Year: 1984
Tongue: English
Weight: 217 KB
Volume: 22
Category: Article
ISSN: 0749-1581
DOI: 10.1002/mrc.1270220606

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✦ Synopsis

Intensity modulated 31P NMR spectra were obtained using the pulse sequence published by Patt and Shoolery. This attached proton test (APT) technique for signal assignment could be applied to systems with long-range heteronuclear couplings in P- 0-C--H fragments. In a model system derived from the alcoholysis of P,sl0 the six reaction products were assigned to the six signals in the "P NMR spectrum.

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