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An improved synthesis of labelled dibromochloropropane

✍ Scribed by O. Buchman; J. Azran; I. Pri-Bar; M. Shimoni

Publisher
John Wiley and Sons
Year
1981
Tongue
French
Weight
294 KB
Volume
18
Category
Article
ISSN
0022-2135

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✦ Synopsis

Abstract

A continuous three‐step micro‐synthesis of 1,2‐dibromo‐3‐chloropropane, labelled with tritium in position 1 and 2, is described. A specific activity of 10.8 Ci/mmol is obtained. The yield observed in the uninterrupted overall synthesis is appreciably lower than that in the controlled step‐by‐step synthesis.

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