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An improved synthesis of [15N] labelled acetamide and acetonitrile

✍ Scribed by D. R. Morgan; H. C. Dorn

Publisher
John Wiley and Sons
Year
1991
Tongue
French
Weight
110 KB
Volume
29
Category
Article
ISSN
0022-2135

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✦ Synopsis

Abstract

An improved synthesis of [^15^N] labelled acetamide and acetonitrile is described which provides these compounds in yields of 85% and 64%, respectively. The key difference in the present preparation is the use of 2,2,2‐trifluoroethyl acetate for the reaction with ^15^NH~4~OH.

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