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Addition of ω-Carboxyalkyl radicals to olefins, synthesis of DI- and trigarboxylic acids

✍ Scribed by E. K. Starostin; B. A. Golovin; G. I. Nikishin

Book ID
112440226
Publisher
Springer
Year
1974
Tongue
English
Weight
284 KB
Volume
23
Category
Article
ISSN
1573-9171

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Addition of methoxy radicals to olefins
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## Abstract The addition of methoxy radicals to several olefins has been studied by a competitive method at 127°C in gas phase. The thermal decomposition of dimethyl peroxide was used as methoxy radical source. The rate of addition to the double bond was measured relative to the oxidation of carbon

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The Bu3SnH -AIBN induced radical additions of 2,3,f+,6-tetra-Oacetyl-D-glucopyranosyl derivatives, bearing c+Br (l), U-1 (5), @OCSSMe (77, and p-SePh (8) groups on the anomeric carbon, with olefins such as dimethyl maleate, methyl vinyl ketone, dimethyl acetylenedicarboxylate, butyl vinyl ether, and