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A simplified route to a key intermediate in the total synthesis of α-onocerin

✍ Scribed by Naftali Danieli; Yehuda Mazur; Franz Sondheimer

Book ID
108383217
Publisher
Elsevier Science
Year
1961
Tongue
French
Weight
114 KB
Volume
2
Category
Article
ISSN
0040-4039

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A novel approach to a key intermediate i
A novel approach to a key intermediate in the total synthesis of α-onocerin
✍ R.F. Church; R.E. Ireland; J.A. Marshall 📂 Article 📅 1961 🏛 Elsevier Science 🌐 French ⚖ 242 KB

The total synthesis of the naturally occurring triterpene aonocerin was first accomplished by Stork and co-workers 3 via the Alternate approach to a-onocerin No. 1 6% yield to the acetoxy ester(lO), m.p. 121-122"(C,70.67$; H, 9.33%) by successive treatment with diazomethane, sodium borohydride and t

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✍ E.J. Corey; Paul Da Silva Jardine; Tetsuya Mohri 📂 Article 📅 1988 🏛 Elsevier Science 🌐 French ⚖ 217 KB

An enantioselective route for the total synthesis of forskolin, a potent activator of adenylate cyclase, has been developed which is based on reduction of dienone 3 to the (S)-alcohol4 and conversion in two steps to tricyclic lactone 9, obtained in optically pure form simply by recrystallization. A