H,SO, bis pH 2 angcsiuert. Der sofort ausfallendc wciOc. rosa schimmernde Niederschlag wird mit 10 mbar uber eine Glasfritte abgesaugt. drei ma1 mit 25 mL Eiswasser uud dreimal mit 25 mL n-Hexan gewaschen und 3 h bei 5 x mbar getrocknet. Ausb. 0.25 g (1.2 mmol, 57%) mil Schmp. 93°C (Zers.
✦ LIBER ✦
A Simple Synthesis of [(Cp*Al)4] and Its Conversion to the Heterocubanes [(Cp*AlSe)4] and [(Cp*AlTe)4] (Cp* = η5-C5(CH3)5)
✍ Scribed by Dipl.-Chem. Stephan Schulz; Prof. Dr. Herbert W. Roesky; Dr. Hans Joachim Koch; Prof. George M. Sheldrick; Dr. Dietmar Stalke; Annja Kuhn
- Publisher
- John Wiley and Sons
- Year
- 1993
- Tongue
- English
- Weight
- 405 KB
- Volume
- 32
- Category
- Article
- ISSN
- 0044-8249
No coin nor oath required. For personal study only.
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