𝔖 Bobbio Scriptorium
✦   LIBER   ✦

A simple synthesis of [11C]methyl triflate

✍ Scribed by Douglas M. Jewett


Publisher
Elsevier Science
Year
1992
Weight
203 KB
Volume
43
Category
Article
ISSN
0883-2889

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✦ Synopsis


[11C]Methyl triflate ([11C]methyl trifluoromethanesulfonate) was formed in high yield when [11C]methyl iodide in a nitrogen carrier was passed at 200 degrees C through a column containing graphitized carbon impregnated with 50% by weight of silver triflate.


πŸ“œ SIMILAR VOLUMES


Simple synthesis of [1-11C]acetate
✍ D. Le Bars; M. Malleval; F. Bonnefoi; C. Tourvieille πŸ“‚ Article πŸ“… 2006 πŸ› John Wiley and Sons 🌐 French βš– 148 KB

## Abstract [1‐^11^C]Acetate is prepared by carboxylation of a Grignard reagent, CH~3~MgBr, on a simple polyethylene loop with cyclotron‐produced [^11^C]carbon dioxide, followed by hydrolysis and purification on solid‐phase extraction cartridges. Copyright Β© 2006 John Wiley & Sons, Ltd.