A simple sterospecific synthesis of 14-hydroxymorphinans
โ Scribed by Zimmerman, M. P.; Gates, M. D.
- Book ID
- 126254916
- Publisher
- American Chemical Society
- Year
- 1982
- Tongue
- English
- Weight
- 438 KB
- Volume
- 47
- Category
- Article
- ISSN
- 0022-3263
No coin nor oath required. For personal study only.
๐ SIMILAR VOLUMES
## Abstract Propionicโ3โ^14^C acid was prepared by methylation of tricarbethoxymethane and subsequent hydrolysis. This method avoids the problems of malonic ester synthesis. A pure monoalkyl derivative was obtained.
## Abstract The reaction of labelled cholesterol with a large excess of freshly prepared 14โmethylhexadecanoyl chloride in a simple glass apparatus was used for the synthesis of [^3^H]cholesteryl 14โmethylhexadecanoate in microgram amounts. After purification of the crude product by thinโlayer chro
## Abstract A synthesis of 1โ^14^Cโacetylhydrazine by acetylation of hydrazine using 1โ ^14^Cโethyl acetate and a catalytic amount of activated alumina is described.