✦ LIBER ✦

A redetermination of [N,N-bis(3,5-dimethyl-1H-pyrazol-1-ylmethyl-κN2)-2-hydroxyethylamine-κN](3,5-dimethyl-1H-pyrazole-κN2)nitratocopper(II) nitrate

✍ Scribed by Ramdani, Abdelkrim ;El Kodadi, Mohamed ;Fouad, Malek ;Eddike, Driss ;Tillard, Monique ;Belin, Claude

Publisher: International Union of Crystallography
Year: 2005
Tongue: English
Weight: 261 KB
Volume: 61
Category: Article
ISSN: 1600-5368
DOI: 10.1107/s1600536805001170

No coin nor oath required. For personal study only.

✦ Synopsis

A redetermination of [N,N-bis(3,5-

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The Cu II atom in the title complex, [Cu(C 12 H 12 N 2 O 3 )-(C 5 H 8 N 2 )], is coordinated by two carboxyl O atoms and one hydrazine N atom from the 4-oxidopent-3-en-2-one 2hydroxybenzoylhydrazone ligand (sph 2À ) and one N atom of 3,5-dimethylpyrazole, forming a distorted square-planar geometry.

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The title compound, [Ti(C 4 H 9 N)Cl(C 5 H 5 N) 2 (C 7 H 11 N 2 )]ÁC 7 H 8 , has a mononuclear structure featuring a six-coordinate distorted octahedral titanium(IV) centre. The central Ti IV ion is coordinated by two N atoms from a dimethyl(1H-pyrrol-2-ylmethyl)amine molecule, two N atoms from two

A redetermination of [N,N-bis(3,5-dimethyl-1H-pyrazol-1-ylmethyl-κN2)-2-hydroxyethyl­amine-κN](3,5-dimethyl-1H-pyrazole-κN2)nitratocopper(II) nitrate

✦ Synopsis

A redetermination of [N,N-bis(3,5-dimethyl-1H-pyrazol-1-ylmethyl-κN2)-2-hydroxyethylamine-κN](3,5-dimethyl-1H-pyrazole-κN2)nitratocopper(II) nitrate