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A one pot, solvent-free synthesis of acyclic α-nitro ketones through the nitroaldol reaction

✍ Scribed by Roberto Ballini; Giovanna Bosica; Mauro Parrini

Book ID
104260008
Publisher
Elsevier Science
Year
1998
Tongue
French
Weight
117 KB
Volume
39
Category
Article
ISSN
0040-4039

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✦ Synopsis

Acyclic ¢z-nitro ketones are easily obtained in one pot, through a solvent-free procedure by nitronldol (Henry) reaction on neutral alumina, then in situ oxidation of the nitroalkanol using wet alumina supported chromium(Vl) oxide.

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✍ R. BALLINI; G. BOSICA; M. PARRINI 📂 Article 📅 2010 🏛 John Wiley and Sons ⚖ 31 KB 👁 1 views

A One Pot, Solvent-Free Synthesis of Acyclic α-Nitro Ketones Through the Nitroaldol Reaction. -Acyclic α-nitro ketones (III) (15 examples) are easily obtained in a one pot reaction in good yields through a solvent-free nitroaldol reaction of nitroalkanes (I) and aldehydes (II) on neutral alumina fo