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ChemInform Abstract: A One Pot, Solvent-Free Synthesis of Acyclic α-Nitro Ketones Through the Nitroaldol Reaction.

✍ Scribed by R. BALLINI; G. BOSICA; M. PARRINI

Publisher
John Wiley and Sons
Year
2010
Weight
31 KB
Volume
30
Category
Article
ISSN
0931-7597

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✦ Synopsis

A One Pot, Solvent-Free Synthesis of Acyclic α-Nitro Ketones Through the Nitroaldol Reaction.

-Acyclic α-nitro ketones (III) (15 examples) are easily obtained in a one pot reaction in good yields through a solvent-free nitroaldol reaction of nitroalkanes (I) and aldehydes (II) on neutral alumina followed by an in situ oxidation of the intermediate nitroalkanols using wet alumina supported chromium(VI) oxide. -(BALLINI, R.; BOSICA, G.;

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