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A novel transformation of 2-acetylthiophene and its halogen derivatives under Vilsmeier reaction conditions

✍ Scribed by Valerii Z. Shirinian; Leonid I. Belen’kii; Mikhail M. Krayushkin

Book ID
119767960
Publisher
Royal Society of Chemistry
Year
2002
Tongue
English
Weight
86 KB
Volume
12
Category
Article
ISSN
0959-9436

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A Novel One-Pot Synthesis of 2-Aminoquinolines from Arylazidoketones by Cyclization under Vilsmeier Conditions. -The reaction of Vilsmeier reagent with 2-azidophenyl ketones is investigated. 1-(2-Azidophenyl)ethanone (I) yields a mixture of the aminoquinolines (III) and (IV). Unexpectedly, the anal