✦ LIBER ✦

A convenient synthesis of [2,6-14C]-2-chloroisonicotinic acid

✍ Scribed by Terence P. Kelly; Thomas R. Rodgers; Christopher Wright

Publisher: John Wiley and Sons
Year: 2001
Tongue: French
Weight: 88 KB
Volume: 44
Category: Article
ISSN: 0022-2135
DOI: 10.1002/jlcr.473

No coin nor oath required. For personal study only.

✦ Synopsis

Abstract

[2,6‐^14^C]‐2‐chloroisonicotinic acid (1) was prepared by kinetically controlled lithiation and carbonation of [2,6‐^14^C]‐2,6‐dichloropyridine, followed by reduction using hydrazine and potassium hydroxide. Copyright © 2001 John Wiley & Sons, Ltd.

📜 SIMILAR VOLUMES

A convenient synthesis of 2 - [14C] - ho

A convenient synthesis of 2 - [14C] - hordenine

✍ George A. Digenis; J. W. Burkett; V. Mihranian 📂 Article 📅 1972 🏛 John Wiley and Sons 🌐 French ⚖ 165 KB

## Abstract A simple and convenient laboratory procedure is described by which hordenine (III), labelled at the carbon residing on the benzene ring, can be synthesized by decarboxylation of 3‐ [^14^C]‐tyrosine (1) and subsequent reductive methylation of the resulting tyramine (II).

Synthesis of 1,2,6,7-14C-chelidonic acid

✍ J. Bergman; J. R. Gear 📂 Article 📅 1975 🏛 John Wiley and Sons 🌐 French ⚖ 126 KB

## Abstract A semimicro synthesis was devised to prepare pure 1,2,6,7‐^14^C‐chelidonic acid of high specific activity from 1,2‐^14^C‐oxalic acid.

Convenient synthesis of [2-14C]-methylgl

Convenient synthesis of [2-14C]-methylglyoxal bis(guanylhydrazone), [14C]-mitoguazone

✍ Alain Burgos; George J. Ellames 📂 Article 📅 1995 🏛 John Wiley and Sons 🌐 French ⚖ 173 KB

## Abstract [2‐^14^C]‐Methylglyoxal bis(guanylhydrazone) dihydrochloride, [^14^C]‐mitoguazone, 3, has been prepared in three steps from potassium [1‐^14^C]‐acetate in an overall radiochemical yield of 16%. The key steps in this procedure are the formation of the sodium salt of [__acetone__‐2‐^14^C]

A simple synthesis of 2, 6-diaminopimeli

A simple synthesis of 2, 6-diaminopimelic-/ 1, 7- 14C/acid

✍ A. Arendt; A. Kolodziejczyk 📂 Article 📅 1973 🏛 John Wiley and Sons 🌐 French ⚖ 152 KB

## Abstract A convenient method of synthesis of 2, 6‐diaminopinelic / 1, 7 ^14^C / acid / DAP / has been elaborated. Glutaric aldehyde and K^14^CN produced the dicyanhydrine which was converted without izolation into the dihydantoine derivative of DAP by treatment with NH~4~HCO~3~. Hydrolisis /H~2~

3, 6-dichloropicolinic acid-2, 6- 14C

✍ L. H. McKendry 📂 Article 📅 1983 🏛 John Wiley and Sons 🌐 French ⚖ 272 KB

## Abstract A 20.4 mCi sample of 99% radiochemically pure 3,6‐dichloropicolinic acid‐2,6‐^14^C with a specific activity of 11.6 mCi/ mmole was synthesized __via__ a five step process from glutarimide‐ 2, 6‐ ^14^C.

Synthesis of nitrilotriacetic acid-2-14C

✍ Michael Bentov; Aharon Levi; Ernst D. Bergmann 📂 Article 📅 1967 🏛 John Wiley and Sons 🌐 French ⚖ 200 KB

Synthesis of Nitrilotriacetic Acid-2-14C