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9-Fluorenylmethoxycarbonyl-Based Solid-Phase Synthesis of Peptide α-Thioesters

✍ Scribed by Dr. Franziska Mende; Prof. Dr. Oliver Seitz

Publisher
John Wiley and Sons
Year
2010
Tongue
English
Weight
710 KB
Volume
50
Category
Article
ISSN
0044-8249

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Base-catalyzed cleavage of the 9-fluorenylmethoxycarbonyl (FMOC) group and subsequent analysis by UV spectrophotometry is commonly employed to measure the ''loading'' of functional groups on solid support. Recent work suggests that 1,8-diazabicyclo[5.4.0]undec-7-ene (DBU) may be superior to piperidi