𝔖 Bobbio Scriptorium
✦   LIBER   ✦

6,6′-Di­chloro-3,3′-(butane-1,4-diyl­dioxy)­diflavone

✍ Scribed by Thinagar, S. ;Velmurugan, D. ;Gupta, S. C. ;Merazig, H. ;Bouacida, S.


Book ID
104479943
Publisher
International Union of Crystallography
Year
2002
Tongue
English
Weight
183 KB
Volume
58
Category
Article
ISSN
1600-5368

No coin nor oath required. For personal study only.

✦ Synopsis


Molecules of the title compound, C 34 H 24 Cl 2 O 6 , lie across crystallographic inversion centres. The ¯avone moiety is slightly folded, with the benzene and dihydropyrone rings making a dihedral angle of 2.5 (2) . In the crystal, the molecules exist as cyclic intermolecular CÐHÁ Á ÁCl hydrogenbonded dimers. The structure is further stabilized by van der Waals interactions.


📜 SIMILAR VOLUMES


(1α,2β,3α,6β)-3,6-Di­chloro­cyclo­hex-4-
✍ Akkurt, Mehmet ;Öztürk, Sema ;Baran, Arif ;Seçen, Hasan ;Büyükgüngör, Orhan 📂 Article 📅 2004 🏛 International Union of Crystallography 🌐 English ⚖ 274 KB

Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.006 A Ê R factor = 0.049 wR factor = 0.145 Data-to-parameter ratio = 9.9 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

2,2′-(1,4-Butane­diyl­di­thio)-1,3-di­th
✍ Xin, Ying ;Liu, Hui-Min ;Zhang, Wei ;Zhang, Wen-Qin 📂 Article 📅 2003 🏛 International Union of Crystallography 🌐 English ⚖ 453 KB

The title compound, C 10 H 14 N 2 S 4 , was synthesized by the reaction of the potassium salt of 2-thiothiazole and 1,4dibromobutane. The two 2-thiazolethio groups are related by a center of symmetry. The plane de®ned by the butyl carbon chain is approximately orthogonal to the thiazole plane, with

(1α,2β,5β,6α)-5,6-Di­chloro-3-cyclo­hexe
✍ Öztürk, Sema ;Akkurt, Mehmet ;Baran, Arif ;Seçen, Hasan ;Büyükgüngör, Orhan 📂 Article 📅 2004 🏛 International Union of Crystallography 🌐 English ⚖ 280 KB

The reaction of endo-cis-7-oxabicyclo[2.2.1]hept-5-ene-2,3diol with BCl 3 followed by acetylation with acetyl chloride gives dichloroconduritol derivatives. The crystal structure of the title compound, C 10 H 12 Cl 2 O 4 , has been investigated. The cyclohexene ring adopts a distorted half-chair con