The reaction of endo-cis-7-oxabicyclo[2.2.1]hept-5-ene-2,3diol with BCl 3 followed by acetylation with acetyl chloride gives dichloroconduritol derivatives. The crystal structure of the title compound, C 10 H 12 Cl 2 O 4 , has been investigated. The cyclohexene ring adopts a distorted half-chair con
(1α,2β,3α,6β)-3,6-Dichlorocyclohex-4-ene-1,2-diyl diacetate
✍ Scribed by Akkurt, Mehmet ;Öztürk, Sema ;Baran, Arif ;Seçen, Hasan ;Büyükgüngör, Orhan
- Publisher
- International Union of Crystallography
- Year
- 2004
- Tongue
- English
- Weight
- 274 KB
- Volume
- 60
- Category
- Article
- ISSN
- 1600-5368
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✦ Synopsis
Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.006 A Ê R factor = 0.049 wR factor = 0.145 Data-to-parameter ratio = 9.9 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
📜 SIMILAR VOLUMES
In the title compound, C 18 H 11 Cl 2 NO 2 , the succinimide and cyclobutene rings are individually planar, with a dihedral angle of 66.02 ( 14) between them. The crystal structure is stabilized by CÐHÁ Á Á% interactions involving the phenyl rings.
In the title molecule, C 24 H 20 N 2 O 5 , the cyclohexene ring adopts a half-chair conformation. The molecular structure shows some intra-and intermolecular hydrogen bonds.
Single-crystal X-ray study T = 150 K Mean '(C±C) = 0.006 A Ê Disorder in main residue R factor = 0.053 wR factor = 0.154 Data-to-parameter ratio = 7.9 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.