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4-N-Acetyl­amino-5-[N-acetyl-N-(tetra-O-acetyl-β-d-glucopyranos­yl)amino]-1,3-dimethyl­uracil

✍ Scribed by Sánchez Rodrigo, Adolfo ;Nogueras Montiel, Manuel ;Cobo, Justo ;Low, John N. ;Glidewell, Christopher

Publisher
International Union of Crystallography
Year
2006
Tongue
English
Weight
318 KB
Volume
62
Category
Article
ISSN
1600-5368

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✦ Synopsis

The title compound, C 24 H 32 N 4 O 13 , crystallizes with two molecules in the asymmetric unit. These have very similar conformations, and each contains an intramolecular N-HÁ Á ÁO hydrogen bond. There are no significant intermolecular interactions.

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✍ Yang, Bo ;Zhang, Shu-Sheng ;Wang, Yang-Fang ;Li, Xue-Mei ;Jiao, Kui 📂 Article 📅 2004 🏛 International Union of Crystallography 🌐 English ⚖ 423 KB

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✍ Röper, Harald ;Heyns, Kurt ;Röper, Siyka ;Meyer, Bernd 📂 Article 📅 1982 🏛 John Wiley and Sons 🌐 English ⚖ 772 KB

## Abstract Durch Umsetzung von 1,3,4,6‐Tetra‐__O__‐acetyl‐β‐D‐glucosamin‐hydrochlorid **(1)** oder 1,3,4,6‐Tetra‐__O__‐acetyl‐β‐D‐galactosamin‐hydrochlorid **(10)** mit Bromcarbonsäure‐methylestern in siedendem Aceton in Gegenwart von Natriumhydrogencarbonat als Base werden die __N__‐(1,3,4,6‐Tetr