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(4-Amino-3-phenyl-5-thioxo-4,5-dihydro-1H-1,2,4-triazol-1-yl)triphenyltin(IV)

✍ Scribed by Wang, Qingfeng ;Zhang, Rufen ;Du, Lingyun


Publisher
International Union of Crystallography
Year
2007
Tongue
English
Weight
377 KB
Volume
63
Category
Article
ISSN
1600-5368

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✦ Synopsis


In the title complex, [Sn(C 6 H 5 ) 3 (C 8 H 7 N 4 S)], all bond lengths and angles show normal values. The Sn centre is fourcoordinated by three C atoms [Sn-C 2.119 (6)-2.133 (6) A ˚] and one N atom [Sn-N 2.107 (5) A ˚] in a distorted tetrahedral geometry. The crystal packing exhibits no classical intermolecular hydrogen bonds.


πŸ“œ SIMILAR VOLUMES


Ethyl (1-methyl-3-phenyl-5-thioxo-4,5-di
✍ Kruszynski, Rafal ;Trzesowska, Agata ;Przybycin, Magdalena ;Dopieralski, Mariusz πŸ“‚ Article πŸ“… 2007 πŸ› International Union of Crystallography 🌐 English βš– 438 KB

All interatomic distances in the title compound, C~13~H~15~N~3~O~2~S, are normal. The 1,2,4-triazole ring is planar and is inclined at 46.50β€…(6)Β° to the phenyl ring. The ethoxycarbonylmethyl group is also close to being planar and is inclined at 87.54β€…(9)Β° to the 1,2,4-triazole ring. The crystal was

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All interatomic distances in the title compound, C~5~H~7~N~3~O~2~S, are normal. The 1,2,4-triazoline ring is planar and it is inclined at 78.61β€…(7)Β° to the planar acetic acid group. The molecules of the title compound are connected __via__ Oβ€”H...N hydrogen bonds into zigzag chains along the [101] di

BisΒ­[4-phenyl-5-(1H-1,2,4-triazol-3-yl)-
✍ Pan, Fu-You ;Yang, Jian-Guo ;Chen, Ding-Ben ;Huang, Ling πŸ“‚ Article πŸ“… 2005 πŸ› International Union of Crystallography 🌐 English βš– 235 KB

The title compound, C 20 H 14 N 12 S 2 , was synthesized by the reaction of 3-hydrazino-1H-1,2,4-triazole with phenyl isocyanate in benzene and by ring closure in an alkaline medium. Intermolecular N-HÁ Á ÁN hydrogen bonds are observed and these form a five-membered ring.

3-Methyl-1-phenyl-4,5-dihydro-1,2,4-tria
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In the molecule of the title compound, C 9 H 9 N 3 O, the dihedral angle between the planar rings is 7.49 (3) . In the crystal structure, intermolecular N-HÁ Á ÁO hydrogen bonds link the molecules into dimers, which may be effective in the stabilization of the crystal structure.

4-Amino-3-(1,2,4-triazol-1-yl)-1H-1,2,4-
✍ Xu, Liang-Zhong ;Yu, Guan-Ping ;Xu, Feng-Ling ;Li, Wei-Hua πŸ“‚ Article πŸ“… 2005 πŸ› International Union of Crystallography 🌐 English βš– 230 KB

In the molecule of the title compound, C 5 H 7 N 7 S, the essentially planar triazole ring and the 4-amino-5-mercapto-1,2,4-triazole moiety make a dihedral angle of 70.97 (5) . In the crystal structure, weak intermolecular N-HÁ Á ÁN and N-HÁ Á ÁS hydrogen bonds stabilize the packing.