✦ LIBER ✦

3-Methyl-1-phenyl-4,5-dihydro-1,2,4-triazol-5(1H)-one

✍ Scribed by Jing, Heng ;Zhu, Hong-Jun ;Liu, Shan ;Zheng, Wei ;Wu, Ya-Ming

Publisher: International Union of Crystallography
Year: 2006
Tongue: English
Weight: 131 KB
Volume: 62
Category: Article
ISSN: 1600-5368
DOI: 10.1107/s1600536806035100

No coin nor oath required. For personal study only.

✦ Synopsis

In the molecule of the title compound, C 9 H 9 N 3 O, the dihedral angle between the planar rings is 7.49 (3) . In the crystal structure, intermolecular N-HÁ Á ÁO hydrogen bonds link the molecules into dimers, which may be effective in the stabilization of the crystal structure.

📜 SIMILAR VOLUMES

Ethyl (1-methyl-3-phenyl-5-thioxo-4,5-di

Ethyl (1-methyl-3-phenyl-5-thioxo-4,5-dihydro-1H-1,2,4-triazol-4-yl)acetate

✍ Kruszynski, Rafal ;Trzesowska, Agata ;Przybycin, Magdalena ;Dopieralski, Mariusz 📂 Article 📅 2007 🏛 International Union of Crystallography 🌐 English ⚖ 438 KB

All interatomic distances in the title compound, C~13~H~15~N~3~O~2~S, are normal. The 1,2,4-triazole ring is planar and is inclined at 46.50 (6)° to the phenyl ring. The ethoxycarbonylmethyl group is also close to being planar and is inclined at 87.54 (9)° to the 1,2,4-triazole ring. The crystal was

1-(Benzoylmethyl)-4-(3,5-dimethyl-4H-1

1-(Benzoylmethyl)-4-(3,5-dimethyl-4H-1,2,4-triazol-4-yl)-3-(2-thienylmethyl)-1H-1,2,4-triazol-5(4H)-one

✍ Sancak, Kemal ;Çoruh, Ufuk ;Ünver, Yasemin ;Vázquez-López, Ezequiel M. 📂 Article 📅 2005 🏛 International Union of Crystallography 🌐 English ⚖ 208 KB

4-Phenyl-3-[(1H-1,2,4-triazol-1-yl)meth

4-Phenyl-3-[(1H-1,2,4-triazol-1-yl)methyl]-1H-1,2,4-triazole-5-thione

✍ Jian, Fang-Fang ;Bai, Zheng-Shuai ;Li, Kai ;Xiao, Hai-Lian 📂 Article 📅 2005 🏛 International Union of Crystallography 🌐 English ⚖ 359 KB

Single-crystal X-ray study T = 295 K Mean '(C±C) = 0.003 A Ê R factor = 0.034 wR factor = 0.084 Data-to-parameter ratio = 12.8 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

1-Methyl-3,5-diphenyl-1H-1,2,4-triazole

✍ Yazıcı, Serap ;Işık, Şamil ;Ağar, Erbil ;Karaoğlu, Şengül Alpay ;Bekircan, Olcay 📂 Article 📅 2004 🏛 International Union of Crystallography 🌐 English ⚖ 191 KB

Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.005 A Ê R factor = 0.051 wR factor = 0.141 Data-to-parameter ratio = 14.9 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

(4-Amino-3-phenyl-5-thioxo-4,5-dihydro-1

(4-Amino-3-phenyl-5-thioxo-4,5-dihydro-1H-1,2,4-triazol-1-yl)triphenyltin(IV)

✍ Wang, Qingfeng ;Zhang, Rufen ;Du, Lingyun 📂 Article 📅 2007 🏛 International Union of Crystallography 🌐 English ⚖ 377 KB

In the title complex, [Sn(C 6 H 5 ) 3 (C 8 H 7 N 4 S)], all bond lengths and angles show normal values. The Sn centre is fourcoordinated by three C atoms [Sn-C 2.119 (6)-2.133 (6) A ˚] and one N atom [Sn-N 2.107 (5) A ˚] in a distorted tetrahedral geometry. The crystal packing exhibits no classical

2-(3-Methyl-5-thioxo-4,5-dihydro-1H-1,2,

2-(3-Methyl-5-thioxo-4,5-dihydro-1H-1,2,4-triazol-4-yl)acetic acid

✍ Kruszynski, Rafal ;Trzesowska, Agata ;Przybycin, Magdalena ;Gil, Kamil ;Dobosz, 📂 Article 📅 2007 🏛 International Union of Crystallography 🌐 English ⚖ 668 KB

All interatomic distances in the title compound, C~5~H~7~N~3~O~2~S, are normal. The 1,2,4-triazoline ring is planar and it is inclined at 78.61 (7)° to the planar acetic acid group. The molecules of the title compound are connected __via__ O—H...N hydrogen bonds into zigzag chains along the [101] di