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2-(3-Methyl-5-thioxo-4,5-dihydro-1H-1,2,4-triazol-4-yl)acetic acid

✍ Scribed by Kruszynski, Rafal ;Trzesowska, Agata ;Przybycin, Magdalena ;Gil, Kamil ;Dobosz, Maria

Publisher
International Union of Crystallography
Year
2007
Tongue
English
Weight
668 KB
Volume
63
Category
Article
ISSN
1600-5368

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✦ Synopsis

All interatomic distances in the title compound, C~5~H~7~N~3~O~2~S, are normal. The 1,2,4-triazoline ring is planar and it is inclined at 78.61 (7)° to the planar acetic acid group. The molecules of the title compound are connected via O—H...N hydrogen bonds into zigzag chains along the [101] direction and by N—H...S hydrogen bonds into a three-dimensional net. In addition, a weak C—H...O hydrogen bond can also be found in the structure.

📜 SIMILAR VOLUMES

Ethyl (1-methyl-3-phenyl-5-thioxo-4,5-di
Ethyl (1-methyl-3-phenyl-5-thioxo-4,5-dihydro-1H-1,2,4-triazol-4-yl)acetate
✍ Kruszynski, Rafal ;Trzesowska, Agata ;Przybycin, Magdalena ;Dopieralski, Mariusz 📂 Article 📅 2007 🏛 International Union of Crystallography 🌐 English ⚖ 438 KB

All interatomic distances in the title compound, C~13~H~15~N~3~O~2~S, are normal. The 1,2,4-triazole ring is planar and is inclined at 46.50 (6)° to the phenyl ring. The ethoxycarbonylmethyl group is also close to being planar and is inclined at 87.54 (9)° to the 1,2,4-triazole ring. The crystal was

(4-Amino-3-phenyl-5-thioxo-4,5-dihydro-1
(4-Amino-3-phenyl-5-thioxo-4,5-dihydro-1H-1,2,4-triazol-1-yl)triphenyltin(IV)
✍ Wang, Qingfeng ;Zhang, Rufen ;Du, Lingyun 📂 Article 📅 2007 🏛 International Union of Crystallography 🌐 English ⚖ 377 KB

In the title complex, [Sn(C 6 H 5 ) 3 (C 8 H 7 N 4 S)], all bond lengths and angles show normal values. The Sn centre is fourcoordinated by three C atoms [Sn-C 2.119 (6)-2.133 (6) A ˚] and one N atom [Sn-N 2.107 (5) A ˚] in a distorted tetrahedral geometry. The crystal packing exhibits no classical

3-Methyl-1-phenyl-4,5-dihydro-1,2,4-tria
3-Methyl-1-phenyl-4,5-dihydro-1,2,4-triazol-5(1H)-one
✍ Jing, Heng ;Zhu, Hong-Jun ;Liu, Shan ;Zheng, Wei ;Wu, Ya-Ming 📂 Article 📅 2006 🏛 International Union of Crystallography 🌐 English ⚖ 131 KB

In the molecule of the title compound, C 9 H 9 N 3 O, the dihedral angle between the planar rings is 7.49 (3) . In the crystal structure, intermolecular N-HÁ Á ÁO hydrogen bonds link the molecules into dimers, which may be effective in the stabilization of the crystal structure.