𝔖 Bobbio Scriptorium
✦   LIBER   ✦

Bis­[4-phenyl-5-(1H-1,2,4-triazol-3-yl)-4H-1,2,4-triazol-3-yl] di­sulfide

✍ Scribed by Pan, Fu-You ;Yang, Jian-Guo ;Chen, Ding-Ben ;Huang, Ling

Publisher
International Union of Crystallography
Year
2005
Tongue
English
Weight
235 KB
Volume
61
Category
Article
ISSN
1600-5368

No coin nor oath required. For personal study only.

✦ Synopsis

The title compound, C 20 H 14 N 12 S 2 , was synthesized by the reaction of 3-hydrazino-1H-1,2,4-triazole with phenyl isocyanate in benzene and by ring closure in an alkaline medium. Intermolecular N-HÁ Á ÁN hydrogen bonds are observed and these form a five-membered ring.

📜 SIMILAR VOLUMES

4-Phenyl-3-[(1H-1,2,4-triazol-1-yl)­meth
4-Phenyl-3-[(1H-1,2,4-triazol-1-yl)­methyl]-1H-1,2,4-triazole-5-thione
✍ Jian, Fang-Fang ;Bai, Zheng-Shuai ;Li, Kai ;Xiao, Hai-Lian 📂 Article 📅 2005 🏛 International Union of Crystallography 🌐 English ⚖ 359 KB

Single-crystal X-ray study T = 295 K Mean '(C±C) = 0.003 A Ê R factor = 0.034 wR factor = 0.084 Data-to-parameter ratio = 12.8 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

3-(1,5-Di­methylpyrazol-4-yl)-4-phenyl-1
3-(1,5-Di­methylpyrazol-4-yl)-4-phenyl-1H-1,2,4-triazole-5(4H)-thione
✍ Wen, Li-Rong ;Ke, Zi-Qin ;Li, Ming ;Guo, Wei-Si 📂 Article 📅 2005 🏛 International Union of Crystallography 🌐 English ⚖ 158 KB

The title compound, C 13 H 13 N 5 S, possesses crystallographically imposed mirror symmetry. In the crystal structure, the molecules interact through strong intermolecular N-HÁ Á ÁN hydrogen bonds to form ribbons running parallel to the a axis.

1-(Acetonyl)-3-(2-thienylmethyl)-4-(4H-1
1-(Acetonyl)-3-(2-thienylmethyl)-4-(4H-1,2,4-triazol-4-yl)-1H-1,2,4-triazol-5(4H)-one
✍ Ustabaş, Reşat ;Çoruh, Ufuk ;Sancak, Kemal ;Demirkan, Esra ;Vázquez-López, Ezequ 📂 Article 📅 2007 🏛 International Union of Crystallography 🌐 English ⚖ 540 KB

In the title compound, C 12 H 12 N 6 O 2 S, the thiophene ring is disordered equally over two positions, corresponding to rotation of approximately 180 about the C-C single bond. The central triazole ring has substituents at the 1-, 3-, 4-and 5positions. Intermolecular C-HÁ Á ÁN and C-HÁ Á ÁO intera

4-Amino-3-(1,2,4-triazol-1-yl)-1H-1,2,4-
4-Amino-3-(1,2,4-triazol-1-yl)-1H-1,2,4-triazole-5(4H)-thione
✍ Xu, Liang-Zhong ;Yu, Guan-Ping ;Xu, Feng-Ling ;Li, Wei-Hua 📂 Article 📅 2005 🏛 International Union of Crystallography 🌐 English ⚖ 230 KB

In the molecule of the title compound, C 5 H 7 N 7 S, the essentially planar triazole ring and the 4-amino-5-mercapto-1,2,4-triazole moiety make a dihedral angle of 70.97 (5) . In the crystal structure, weak intermolecular N-HÁ Á ÁN and N-HÁ Á ÁS hydrogen bonds stabilize the packing.