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3-Methoxy­carbonyl-1-methyl­pyridinium bis(2-thio­xo-1,3-di­thiole-4,5-di­thiol­ato)­nickelate(II)

✍ Scribed by Tomono, Kazuaki ;Sasaki, Yuka ;Miyamura, Kazuo

Publisher
International Union of Crystallography
Year
2004
Tongue
English
Weight
230 KB
Volume
61
Category
Article
ISSN
1600-5368

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✦ Synopsis

Single-crystal X-ray study T = 100 K Mean '(C±C) = 0.009 A Ê R factor = 0.064 wR factor = 0.185 Data-to-parameter ratio = 19.1 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

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In the title complex, (C 6 H 8 N) 2 [Zn(dmit) 2 ] (dmit is 2-thioxo-1,3-dithiole-4,5-dithiolate, C 3 S 5 ), each Zn atom is coordinated by four dmit S atoms that define a distorted tetrahedral arrangement. The crystal structure is stabilized by C-HÁ Á ÁS hydrogen bonding and SÁ Á ÁS contacts.