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3-Cyclo­hexyl-4-(3-methyl-3-phenyl­cyclo­butyl)-1,3-thia­zole-2(3H)-thione

✍ Scribed by Kırılmış, Cumhur ;Koca, Murat ;Arıcı, Cengiz ;Heinemann, Frank W. ;Ahmedzade, Misir

Publisher
International Union of Crystallography
Year
2005
Tongue
English
Weight
128 KB
Volume
61
Category
Article
ISSN
1600-5368

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✦ Synopsis

The cyclohexyl ring of the title compound, C 20 H 25 NS 2 , has a chair conformation. The dihedral angle between the thiazole and phenyl rings is 89.70 (2) . The crystal structure involves two weak intramolecular C-HÁ Á ÁS hydrogen-bond contacts.

📜 SIMILAR VOLUMES

3-Butyl-4-(3-methyl-3-phenyl­cyclo­but-1
3-Butyl-4-(3-methyl-3-phenyl­cyclo­but-1-yl)-1,3-thia­zole-2(3H)-thione
✍ Kırılmış, Cumhur ;Koca, Murat ;Arıcı, Cengiz ;Heinemann, Frank W. ;Ahmedzade, Mi 📂 Article 📅 2005 🏛 International Union of Crystallography 🌐 English ⚖ 117 KB

In the title compound, C 18 H 23 NS 2 , the bond lengths and angles are unexceptional. The butyl chain is in a fully extended conformation. The dihedral angle between the thiazole and phenyl rings is 87.21 (2) . The crystal structure is stabilized by one weak intramolecular C-HÁ Á ÁS hydrogen bond.

5-(4-Methoxy­phenyl)-4-methyl­thia­zole-
5-(4-Methoxy­phenyl)-4-methyl­thia­zole-2(3H)-thione
✍ Hartung, Jens ;Daniel, Kristina ;Svoboda, Ingrid ;Fuess, Hartmut 📂 Article 📅 2005 🏛 International Union of Crystallography 🌐 English ⚖ 138 KB

The molecules of the title compound, C 11 H 11 NOS 2 , form hydrogen-bonded dimers in the solid state. The amide H atom serves as hydrogen-bond donor and the thiocarbonyl S atom of a neighbouring molecule serves as acceptor. The pmethoxyphenyl substituent is tilted by 7.3 (5) from the thiazole-2(3H)

5-Amino-1,3-benzo­thia­zole-2(3H)-thione
5-Amino-1,3-benzo­thia­zole-2(3H)-thione
✍ Zhong, Hui-Ping ;Long, La-Sheng ;Huang, Rong-Bin ;Zheng, Lan-Sun ;Ng, Seik Weng 📂 Article 📅 2003 🏛 International Union of Crystallography 🌐 English ⚖ 158 KB

Single-crystal X-ray study T = 298 K Mean '(C±C) = 0.004 A Ê R factor = 0.056 wR factor = 0.125 Data-to-parameter ratio = 15.8 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.