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1-(3-Methyl-3-phenyl­cyclo­butyl)-2-(piperidin-1-yl)ethanone oxime

✍ Scribed by Dinçer, Muharrem ;Özdemir, Namık ;Çukurovalı, Alaaddin ;Yılmaz, İbrahim ;Büyükgüngör, Orhan


Publisher
International Union of Crystallography
Year
2005
Tongue
English
Weight
239 KB
Volume
62
Category
Article
ISSN
1600-5368

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1-(3-Mesit­yl-3-methyl­cyclo­but­yl)-2-(
✍ Çukurovalı, Alaaddin ;Özdemir, Namık ;Yılmaz, İbrahim ;Dinçer, Muharrem 📂 Article 📅 2005 🏛 International Union of Crystallography 🌐 English ⚖ 263 KB

In the title compound, C 21 H 31 NO, the cyclobutane ring is puckered, with a dihedral angle of 25.74 (6) . The mesityl and 2-N-piperidino-1-oxoethyl groups are in cis positions. The piperidine fragment adopts a chair conformation. Intermolecular C-HÁ Á ÁO interactions involving the piperidine CH gr

(2E)-2-(1-Methyl­piperidin-2-yl­idene)-1
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Single-crystal X-ray study T = 173 K Mean (C-C) = 0.003 A Disorder in main residue R factor = 0.051 wR factor = 0.199 Data-to-parameter ratio = 13.3 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

3-Butyl-4-(3-methyl-3-phenyl­cyclo­but-1
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In the title compound, C 18 H 23 NS 2 , the bond lengths and angles are unexceptional. The butyl chain is in a fully extended conformation. The dihedral angle between the thiazole and phenyl rings is 87.21 (2) . The crystal structure is stabilized by one weak intramolecular C-HÁ Á ÁS hydrogen bond.

1-(3-Mesityl-3-methyl­cyclo­butyl)-2-(py
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In the title molecule, C 20 H 29 NO, the cyclobutane ring is puckered, with a dihedral angle of 19.8 (3) between the two planes. The pyrrolidine ring adopts an envelope conformation. There are intermolecular CÐHÁ Á ÁO and CÐHÁ Á Á% interactions.