𝔖 Bobbio Scriptorium
✦   LIBER   ✦

2-Nitro-1-(phenylsulfonyl)-1H-indole

✍ Scribed by Roy, Sujata ;Gribble, Gordon W. ;Jasinski, Jerry P.

Publisher
International Union of Crystallography
Year
2007
Tongue
English
Weight
104 KB
Volume
63
Category
Article
ISSN
1600-5368

No coin nor oath required. For personal study only.

📜 SIMILAR VOLUMES

6-Nitro-1-(phenyl­sulfon­yl)-1H-indole
6-Nitro-1-(phenyl­sulfon­yl)-1H-indole
✍ Kishbaugh, Tara ;Pelkey, Erin T. ;Gribble, Gordon W. ;Jasinski, Jerry P. 📂 Article 📅 2006 🏛 International Union of Crystallography 🌐 English ⚖ 146 KB

In the title compound, C 14 H 10 N 2 O 4 S, the nitro group, confirmed as being in the 6-position, is coplanar with the indole ring system and the angle between the planes of the indole system and the phenyl ring is 96.1 (1) .

3-Nitro-1-(phenyl­sulfon­yl)-1H-indole
3-Nitro-1-(phenyl­sulfon­yl)-1H-indole
✍ Roy, Sujata ;Pelkey, Erin T. ;Gribble, Gordon W. ;Jasinski, Jerry P. 📂 Article 📅 2007 🏛 International Union of Crystallography 🌐 English ⚖ 166 KB

The crystal structure of the title compound, C 14 H 10 N 2 O 4 S, confirms the position of the nitro group at position C-3 of the indole ring system. While the nitro group is coplanar with the indole ring system, the angle between the indole and phenyl planes is 83.9 (3) .

3-Benzyl-2-methyl-1-phenyl­sulfonyl-1H-i
3-Benzyl-2-methyl-1-phenyl­sulfonyl-1H-indole
✍ Malathy Sony, S. M. ;Palani, K. ;Charles, P. ;Ponnuswamy, M. N. ;Sureshbabu, N. 📂 Article 📅 2005 🏛 International Union of Crystallography 🌐 English ⚖ 236 KB
3-Bromo-2-bromo­methyl-1-phenyl­sulfonyl
3-Bromo-2-bromo­methyl-1-phenyl­sulfonyl-1H-indole
✍ Sakthivel, P. ;Sethusankar, K. ;Sankar, P. Jai ;Joseph, P. S. 📂 Article 📅 2007 🏛 International Union of Crystallography 🌐 English ⚖ 160 KB

The phenyl ring in the title compound, C~15~H~11~Br~2~NO~2~S, makes a dihedral angle of 81.8 (1)° with the mean plane of the indole system. The molecular structure is stabilized by C—H...O hydrogen bonds.

2-Methyl-1-phenyl­sulfonyl-1H-indole-3-c
2-Methyl-1-phenyl­sulfonyl-1H-indole-3-carbonitrile
✍ Sakthivel, P. ;Sethusankar, K. ;Jai Shankar, P. ;Joseph, P. S. 📂 Article 📅 2007 🏛 International Union of Crystallography 🌐 English ⚖ 157 KB

To a stirred solution of aluminium chloride (20 mmol) in dry tetrahydrofuran (100 ml), sodium azide (60 mmol) and 1-phenylsulfonyl-