1H-NMR Study of the Di-Glucopyranoses in D2O
โ Scribed by A. De Bruyn; M. Anteunis; G. Verhegge
- Publisher
- Wiley (John Wiley & Sons)
- Year
- 2010
- Weight
- 426 KB
- Volume
- 84
- Category
- Article
- ISSN
- 0037-9646
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## Abstract Complete analyses of the ^1^H n.m.r. spectra at 300 MHz of D~2~0 solutions of 2โdeoxyโDโarabinoโhexopyranose, 2โdeoxyโDโlyxoโhexopyranose and 2โฒโdeoxy lactose. Chemical shifts in the deoxy monosaccharides and in 2โฒโdeoxy lactose are compared with those previously obtained in the parent
## 13 C spin-lattice NMR relaxation rates of pyridine and 4-,3-and 2-aminopyridine were measured in CDCl 3 -DMF and water in the neutral and protonated forms. The relaxation data were analysed in terms of the existence of tight pairs of ions between chloride and protonated pyridine and aminopyridi