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1H-filtered correlation experiments for assignment and determination of coupling constants in backbone labelled proteins

✍ Scribed by Alexander W. Giesen; Lynnette C. Bae; Christa L. Barrett; Jason A. Chyba; Michael M. Chaykovsky; Minn-Chang Cheng; Jenny H. Murray; Ed J. Oliver; Sarah M. Sullivan; Jonathan Miles Brown; Steve W. Homans


Book ID
110324612
Publisher
Springer Netherlands
Year
2002
Tongue
English
Weight
115 KB
Volume
22
Category
Article
ISSN
0925-2738

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A set of three improved two-dimensional (2D) NMR methods for measuring one-bond 15 N-1 H coupling constants in the protein backbone is presented. They are tailored to suit the size of the TROSY effect, i.e., the degree of interference between dipolar and chemical shift anisotropy relaxation mechanis