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Assignment and sign determination of (C, H) and (H, H) coupling constants in N-acetylimidazole with selective population inversion experiments

โœ Scribed by K. G. R. Pachler; P. L. Wessels


Book ID
118285287
Publisher
John Wiley and Sons
Year
1980
Tongue
English
Weight
498 KB
Volume
13
Category
Article
ISSN
0749-1581

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Determination of HN,Hฮฑand HN,Cโ€ฒ coupling
โœ R. Weisemann; H. Rรผterjans; H. Schwalbe; J. Schleucher; W. Bermel; C. Griesinger ๐Ÿ“‚ Article ๐Ÿ“… 1994 ๐Ÿ› Springer Netherlands ๐ŸŒ English โš– 603 KB

Sensitive three-dimensional NMR experiments, based on the E.COSY principle, are presented for the measurement of the 3J(HN, H~) and 3J(HN,C') coupling constants in uniformly 13C-and 15N-labeled proteins. They employ gradient coherence selection in combination with the sensitivity enhancement method