The 1 H and 13 C NMR resonances of 12 tetracyclic phenothiazine derivatives were completely and unequivocally assigned by the concerted application of 1 H-detected heteronuclear one-bond (gs-HMQC) and long-range (gs-HMBC) gradient selected correlation experiments. 1 H and 13 C chemical shifts are al
1H and 13C NMR spectral assignments of some phenothiazine derivatives
✍ Scribed by M. Pelecanou; E. Mikros; P. Catsoulacos
- Publisher
- John Wiley and Sons
- Year
- 1994
- Tongue
- English
- Weight
- 273 KB
- Volume
- 32
- Category
- Article
- ISSN
- 0749-1581
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✦ Synopsis
Abstract
^1^H and ^13^C NMR data for six pheno‐thiazine derivatives are reported. Spectral assignments were made on the basis of two‐dimensional homonuclear ^1^H,^1^H and heteronuclear ^1^H,^13^C correlation techniques (COSY, COSY‐LR, HETCOR, COLOC) and ^13^C,^1^H coupling constant measurements.
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