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1H and 13C NMR spectral assignment of androstane derivatives

✍ Scribed by Ariadna Fuente; Mayra Reyes; Yoanna M. Alvarez; José A. Ruiz; Hermán Vélez; Omar Viñas-Bravo; Sara Montiel-Smith; Socorro Meza-Reyes; Jesús Sandoval-Ramírez

Publisher
John Wiley and Sons
Year
2005
Tongue
English
Weight
80 KB
Volume
43
Category
Article
ISSN
0749-1581

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✦ Synopsis

H and 13 C NMR spectroscopic data for 5a-androstanes and halo-5a-androstanes with different substituents at positions C-3, C-9, C-11 and C-17 were examined and assigned by a combination of 1D and 2D NMR experiments. The substituent effects on the 13 C chemical shifts were compared with those of epi-androsterone, used as a reference compound. The coupling constants n J( 19 F, 13 C) were measured for compounds 6, 8, 11 and 14.

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