𝔖 Bobbio Scriptorium
✦   LIBER   ✦

Complete 1H and 13C NMR spectral assignment of hydrogenated oxoisoaporphine derivatives

✍ Scribed by Eduardo Sobarzo-Sánchez; Bruce K. Cassels; Luis Castedo

Publisher
John Wiley and Sons
Year
2003
Tongue
English
Weight
94 KB
Volume
41
Category
Article
ISSN
0749-1581

No coin nor oath required. For personal study only.

✦ Synopsis

Abstract

2,3,8,9,10,11‐Hexahydro‐7__H__‐dibenzo[de,h]quinolin‐7‐one, 5‐methoxy‐2,3,8,9,10,11‐hexahydro‐7__H__‐dibenzo[de,h]quinolin‐7‐one, 5‐methoxy‐6‐hydroxy‐1,2,3,7a,8,9,10,11,11a,11b‐decahydro‐7__H__‐dibenzo[de,h]quinolin‐7‐one, 5‐methoxy‐5,6,8,9,10,11‐hexahydro‐4__H__‐dibenzo[de,h]quinolin‐7‐ol, 5,6,8,9,10,11‐hexahydro‐4__H__‐dibenzo[de,h]quinolin‐7‐ol and 5,6‐dihydro‐4__H__‐dibenzo[de,h]quinolin‐7‐ol were prepared by catalytic hydrogenation of oxoisoaporphines or their 2,3‐dihydro derivatives over PtO~2~ in acetic acid under mild conditions. Their structures were confirmed and ^1^H and ^13^C NMR spectra were completely assigned using a combination of one‐ and two‐dimensional NMR techniques. Copyright © 2003 John Wiley & Sons, Ltd.

📜 SIMILAR VOLUMES

Complete assignments 1H and 13C NMR spec
Complete assignments 1H and 13C NMR spectral data of four anabaseine derivatives
✍ Eduardo Sobarzo-Sánchez; Julio De la Fuente; Elías Quezada; Luis Castedo 📂 Article 📅 2006 🏛 John Wiley and Sons 🌐 English ⚖ 103 KB 👁 1 views

## Abstract The anabaseine derivatives 6‐methoxy‐7‐hydroxy‐1‐(pyridin‐3‐yl)‐3,4‐dihydroisoquinoline, 6,7‐dimethoxy‐1‐(pyridin‐3‐yl)‐1,2,3,4‐tetrahydroisoquinoline and 6,7‐dimethoxy‐1‐(piperidin‐3‐yl)‐1,2,3,4‐tetrahydroisoquino‐ line were prepared either by demethylation with HBr or by reduction wit

1H and 13C NMR spectral assignment of an
1H and 13C NMR spectral assignment of androstane derivatives
✍ Ariadna Fuente; Mayra Reyes; Yoanna M. Alvarez; José A. Ruiz; Hermán Vélez; Omar 📂 Article 📅 2005 🏛 John Wiley and Sons 🌐 English ⚖ 80 KB

H and 13 C NMR spectroscopic data for 5a-androstanes and halo-5a-androstanes with different substituents at positions C-3, C-9, C-11 and C-17 were examined and assigned by a combination of 1D and 2D NMR experiments. The substituent effects on the 13 C chemical shifts were compared with those of epi-

Complete 1H and 13C NMR spectral assignm
Complete 1H and 13C NMR spectral assignment of symmetric and asymmetric bis-spiropyran derivatives
✍ Sam-Rok Keum; Hyo-Jung Roh; Yoon-Ki Choi; Soon-Sung Lim; Sung-Hoon Kim; Kwangnak 📂 Article 📅 2005 🏛 John Wiley and Sons 🌐 English ⚖ 99 KB

(1)H and (13)C NMR spectra of symmetric and asymmetric bis-spiropyrans, Series 1-3, were completely assigned. Especially, the (1)H assignment of asymmetric spiropyrans was achieved by utilizing (1)H-(1)H COSY and nOe experiments. All of the carbons in the dye molecules were investigated through a co

1H and 13C NMR spectral assignments of s
1H and 13C NMR spectral assignments of some phenothiazine derivatives
✍ M. Pelecanou; E. Mikros; P. Catsoulacos 📂 Article 📅 1994 🏛 John Wiley and Sons 🌐 English ⚖ 273 KB

## Abstract ^1^H and ^13^C NMR data for six pheno‐thiazine derivatives are reported. Spectral assignments were made on the basis of two‐dimensional homonuclear ^1^H,^1^H and heteronuclear ^1^H,^13^C correlation techniques (COSY, COSY‐LR, HETCOR, COLOC) and ^13^C,^1^H coupling constant measurements.

1H and 13C NMR spectral assignment of ph
1H and 13C NMR spectral assignment of phytochelatin
✍ Etsuro Yoshimura; Rinya Kobayashi; Kazuo Furihata; Hideyuki Kajiwara; Sunao Yama 📂 Article 📅 2000 🏛 John Wiley and Sons 🌐 English ⚖ 40 KB 👁 3 views

1 H and 13 C NMR spectral data for phytochelatin, NH 3 C --Glu-Cys 2 -Gly-COO , were assigned by a combination of one-( 1 H, 13 C) and two-dimensional (DQF-COSY, CH-COSY, HMBC) NMR experiments.

1H and 13C NMR Spectral Assignment of St
1H and 13C NMR Spectral Assignment of Strychnobrasiline
✍ Marie-Thérèse Martin; François Frappier; Philippe Rasoanaivo; Milijaona Randrian 📂 Article 📅 1996 🏛 John Wiley and Sons 🌐 English ⚖ 261 KB 👁 2 views

The indole alkaloid strychnobrasiline was studied using one-and two-dimensional NMR techniques. The interpretation of these spectra led to the complete assignments of all carbon and proton chemical shifts.