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1H and 13C NMR spectral assignments of some tetracyclic phenothiazine derivatives

✍ Scribed by F. Chatel; R. Faure; G. Boyer; J. P. Galy

Publisher: John Wiley and Sons
Year: 2000
Tongue: English
Weight: 53 KB
Volume: 38
Category: Article
ISSN: 0749-1581
DOI: 10.1002/(sici)1097-458x(200002)38:2<137::aid-mrc596>3.0.co;2-7

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✦ Synopsis

The 1 H and 13 C NMR resonances of 12 tetracyclic phenothiazine derivatives were completely and unequivocally assigned by the concerted application of 1 H-detected heteronuclear one-bond (gs-HMQC) and long-range (gs-HMBC) gradient selected correlation experiments. 1 H and 13 C chemical shifts are also reported for the respective diphenylamine precursors.

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